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Adiabatic Batch Reactor


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Adiabatic Batch Reactor

Adiabatic Batch Reactor

Technical Description:

An adiabatic batch reactor is a closed system with no input and output streams. This reactor is operated under conditions like adiabatic (Temperature of Reaction Mass keep on changing), perfectly mixed (composition of reaction mixture is uniform throughout), and constant volume (volume of the reaction mixture within the reactor remains constant, there is no appreciable change in the density of reaction mass).

This set-up is used to study a catalytic homogeneous reaction under adiabatic condition. The set-up consists of a Dewar flask of capacity 1 lit. fitted with a stirrer. The flask is double insulated by ceramic wool insulation. Temperature is measured by digital temp indicator. The whole setup is mounted on a rigid M.S. frame.

Technical Specifications:

  Reactor: Material Stainless Steel, Capacity 1 Ltrs. (Approx) Insulated with Ceramic wool.
  Stirrer :Ptfe Impeller and Stainless Steel shaft coupled with FHP motor
  Temperature Sensors: RTD PT-100 type.
  The whole set-up is ingeniously designed and schematically arranged on a powder-coated rigid structure.
 
Control Panel:

  Digital Temp. Indicator : 0-199.9°C, RTD PT-100 type 
  Standard make on/off switch, Mains Indicator etc.
  Temp. Sensors : RTD PT-100 type 

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Experiment

 Learning Objectives/Experiments:

  To study the hydrolysis of acetic an hydride with water in presence of an acid catalyst (H2SO4). 
  To predict the degree of conversion from time-temperature data.
 
Requirement:

  Instruments, Laboratory wares and Chemicals required for analysis as per the system adopted.